View PDF HTML (experimental) Abstract: The widespread adoption of the Internet of Things (IoT) has positioned smart homes as paradigmatic examples of distributed automation systems, where reliability, efficiency, and interoperability depend critically on the underlying communication protocol. Among the low-power wireless technologies available for this scenario, Zigbee and Matter over Thread have emerged as leading contenders. While Zigbee represents a mature, non-IP mesh networking solution, Matter over Thread introduces an IP-based architecture designed to unify device interoperability across different ecosystems. However, despite extensive documentation of their design principles, there is a lack of empirical, comparative performance data under realistic network conditions. This paper presents a comprehensive experimental comparison between the two protocols, conducted on a testbed built from commercially available hardware.…